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Atypical coupling method for the preparation of 1, 2-di (thiophen-2-yl) ethene-1, 2-diol compounds via a cu (ii) catalyst
(
justia patents
, 2022 , Other)
Presented herein is a coupling method for the preparation of 1,2 -di ( thiophen - 2 -yl ) ethane -1,2 -diol compounds, including ( E )-1,2 -di(thiophen - 2 -yl )ethene - 1,2 -diol, via a Cu (II ) catalyst .
l-Proline-Catalyzed Three-Component Reaction of 4-Chloro-3-formylcoumarin, Sodium Sulfide, and α-Halo Ketones: A Direct Approach to Thieno[3,2- c ]coumarins
(
Georg Thieme Verlag KG
, 2023 , Other)
A new protocol for the synthesis of thieno[3,2-c]coumarins is disclosed. In this method, a 3-formyl-2-oxo-2H-chromene-4-thiolate anion is generated in situ by treatment of 4-chloro-3-formylcoumarin with sodium sulfide. ...